Chemistry Letters p. 1095 - 1096 (1999)
Update date:2022-08-10
Topics:
Kongkathip, Boonsong
Sookkho, Rongsan
Kongkathip, Ngampong
Taylor, Walter C.
Both diastereoisomers of 1,4-dimethyl-2,8-dioxabicyclo[3.2.1]octane-4-caboxylic acid ester (3, 4) and the 4-hydroxy methyl analogues (5, 6) were synthesised from ethyl acetoacetate and diethyl malonate respectively. The key step of these process involved intramolecular cyclisation using palladium chloride as catalyst.
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