Journal of Heterocyclic Chemistry p. 727 - 730 (1996)
Update date:2022-08-28
Topics:
Halverson, Aileen Pfleider
Castle, Lyle W.
The synthesis of [1]benzothieno[2,3-c][l,10]phenanthroline (5) is described. It was obtained in four steps from known starting materials. The basic skeleton of the molecule and of the phenanthroline ring were formed via photocyclization. The total assignment of 1H-nmr spectra was accomplished with the aid of two-dimensional nmr methods.
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