Journal of Organic Chemistry p. 2677 - 2682 (1995)
Update date:2022-08-10
Topics:
Kawakami, Takayo
Sugimoto, Takayuki
Shibata, Ikuya
Baba, Akio
Matsuda, Haruo
Sonoda, Noboru
The highly coordinated tin hydride, Bu2SnClH-HMPA (B), is shown to be an effective agent for the reduction of imines.The subsequent alkylation of the resulting intermediate tin amides permitted the preparation of a series of tertiary amines in a one-pot procedure.The spectral identification of the novel tin hydrides, B and Bu2SnClH-Bu4NF, was accomplished by 1H, 13C, and 119Sn NMR and FT-IR studies.
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