Tetrahedron p. 5439 - 5450 (1994)
Update date:2022-08-17
Topics:
Macias
Macias, Francisco A.
Aguilar
Aguilar, Jose Maria
Molinillo
Molinillo, Jose Maria G.
Massanet
Massanet, Guillermo M.
Fronczek
Fronczek, Frank R.
The first approach to the synthesis of decipienin A (1) having the stereostructure b (11β-angeloyloxy-α-santonin) have been performed following three different synthetic routes. The key step on the synthetic procedures is the stereoselective hydroxylation at C-11 position. An evaluation of the different used routes is discussed. Comparison of spectroscopic data of compound 1b and those from the natural decipienin A suggests that a stereostructure type a could be assigned to the natural product.
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