Organic Letters p. 569 - 572 (2005)
Update date:2022-08-11
Topics:
Semmelhack, Martin F.
Campagna, Shawn R.
Federle, Michael J.
Bassler, Bonnie L.
(Chemical Equation Presented) A practical synthesis has been developed for DPD (4,5-dihydroxypentane-2,3-dione), an unstable small molecule that is proposed to be the source of universal signaling agents for quorum sensing in bacteria. The synthesis allows preparation of isotopically labeled DPD and ent-DPD as well as detailed studies of spontaneous binding to borate to give the unusual borate complex 6, the signal for marine bacteria such as Vibrio harveyi.
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