Journal of Organic Chemistry p. 3649 - 3652 (1982)
Update date:2022-08-17
Topics:
Belanger, J.
Landry, N. L.
Pare, J. R.
Jankowski, K.
The thermal condensation of five trimethylsilyloxy 1,3-dienes with ethyl mesoxalate led to dihydropyran adducts.The trimethylsilyloxy radical was then removed by hydrolysis.The Danishefsky diene 1 was used to synthesize, with acetaldehyde, the 2,3-dihydro-2-methyl-4-pyrone (18), which was also obtained by two other independent ways.
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(1984)
