Tetrahedron Letters p. 5479 - 5482 (1988)
Update date:2022-08-11
Topics:
Andrus, Alex
Beaucage, Serge L.
An equimolar (1.5 M) solution of 2-mercaptobenzothiazole and N,N-diisopropylethylamine in 1-methyl-2-pyrrolidinone efficiently removed the methyl phosphate protecting groups from deoxynucleotide phosphotriesters and yielded synthetic oligomers of high genetic integrity.This odorless reagent can therefore substitute for hazardous thiophenol usually used for this purpose.
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