Tetrahedron p. 55 - 60 (2002)
Update date:2022-08-30
Topics:
Paredes, Rodrigo
Abonia, Rodrigo
Cadavid, John
Moreno-Fuquen, Rodolfo
Jaramillo, Alonso
Hormaza, Angelina
Ramirez, Alfonso
Kennedy, Allan
Ammonolysis of alkyl acetoacetates with 15% NH3 in water at room temperature initially lead to formation of alkyl β-aminocrotonates which slowly converted into 1,5-dimethyl-2,6,9-triaza-bicyclo[3.3.1]nonane-3,7-dione as the main product.
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(2001)
