Tetrahedron Letters p. 61 - 64 (1994)
Update date:2022-08-28
Topics:
Wustrow, David J.
Smith, William J.
Wise, Lawrence D.
A series of cyclic secondary allylic alcohols and acetates was deoxygenated using triethylsilane in the presence of ethereal lithium perchlorate.Under these conditions the allylic oxygen functionality was selectively removed in the presence of esters, isolated olefins, ketals and tertiary alcohols.Primary allylic alcohols were not deoxygenated under these conditions.
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