PHOTOSENSITIZED SINGLE ELECTRON TRANSFER OXIDATION OF N-HYDROXYLAMINES: A CONVENIENT SYNTHESIS OF CYCLIC NITRONES

DOI: 10.1016/S0040-4039(00)96172-0

Source and publish data:

Tetrahedron Letters p. 2649 - 2652 (1987)

Update date:2022-08-16

Topics:

Authors:

Pandey, G.

Kumaraswamy, G.

Krishna, A.

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Article abstract of DOI:10.1016/S0040-4039(00)96172-0

Photolysis of N-hydroxylamines of type 1 in the presence of 1,4-dicyanonaphthalene (DCN) as an electron acceptor gave high yields of nitrones 2.Crude nitrones have been trapped by 1,3-dipolar cycloaddition reaction with dimethyl fumarate.Mechanistic pathways have also been discussed.

Full text of DOI:10.1016/S0040-4039(00)96172-0

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