Journal of Fluorine Chemistry p. 63 - 68 (1993)
Update date:2022-08-10
Topics:
Martin, Valerie
Molines, Huguette
Wakselman, Claude
A three-step synthesis of 1-bromo-3-trifluoromethylbut-2-ene in 54percent overall yield is reported starting from 1,1,1-trifluoroacetone.The electrophilic reactivity of this compound towards various nucleophiles has been studied.Thus, for example, condensation with the sodium salt of diethyl malonate gave ethyl 2-carboethoxy-5-trifluoromethylhex-4-enoate in 66percent yield.
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