Tetrahedron Letters p. 7749 - 7752 (1999)
Update date:2022-08-28
Topics:
Davis, D. Scott
Shadinger, Sylvia C.
Various dicobalt hexacarbonyl acetylene complexes were efficiently converted to the unprotected acetylene by the reaction of two molar equivalents of sodium methylthiolate. Yields and reaction times depend upon the choice of solvent. DMF proved to be the
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