A new access to 2-(chloromethyl)acrylonitrile

Article abstract of DOI:10.1080/00397919508013856

An efficient method for the preparation of 2-(chloromethyl)acrylonitrile (7) is reported. The Mannich reaction of cyanoacetic acid with paraformaldehyde and morpholine afforded the allylic amine 6a which was converted into the chloride 7 on treatment with isobutyl chloroformate at room temperature.

Full text of DOI:10.1080/00397919508013856

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Synthetic Communications: An
International Journal for Rapid
Communication of Synthetic
Organic Chemistry
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A New Access to 2-
(
Chloromethyl)acrylonitryle
a
Henryk Krawczyk
a
Institute of Organic Chemistry, Technical University
(Politechnika), 90-924, Łódź, Żwirki 36, Poland
Published online: 23 Sep 2006.
To cite this article: Henryk Krawczyk (1995) A New Access to 2-
(
Chloromethyl)acrylonitryle, Synthetic Communications: An International Journal
for Rapid Communication of Synthetic Organic Chemistry, 25:21, 3357-3362, DOI:
0.1080/00397919508013856
1
To link to this article: http://dx.doi.org/10.1080/00397919508013856
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