Synthetic Communications p. 321 - 326 (2006)
Update date:2022-08-22
Topics:
Curtis, Michael P.
Bunnelle, William H.
Pagano, Thomas G.
Gopalakrishnan, Murali
Faghih, Ramin
Small heterocyclic amines such as 1,3-diaza-bicyclo[3.2.2]nonane are known to be key components of biologically active molecules. A convenient synthesis of this compound utilizing a key Beckmann rearrangement of (Z)-1-aza-bicyclo[2.2. 2]octan-3-one oxime (6) with conc. H2SO4 under microwave irradiation was achieved. The desired compound (1) was obtained in 20% yield overall. Copyright Taylor & Francis LLC.
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