Synthesis p. 2535 - 2538 (2009)
Update date:2022-08-11
Topics:
Hill, Lawrence
Imam, S. Haider
McNab, Hamish
O'Neill, William J.
Flash vacuum pyrolysis (FVP) of tert-butyl {[(2,2-dimethyl-4,6-dioxo-1,3- dioxan-5-ylidene)methyl]amino}acetate at 600°C gives the unstable 3-hydroxy-1H-pyrrole in ca. 55% yield as the only significant product. It exists as the enol tautomer in dimethyl s
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