Improved preparation of 24-crown-8

Article abstract of DOI:10.1080/00397919908085989

An improved method for the preparation of 24-crown-8 is described. Cyclization at room temperature and purification of the crude product via an acetonitrile complex provides a much higher yield than those reported in the literature.

Full text of DOI:10.1080/00397919908085989

Synthetic Communications
ISSN: 0039-7911 (Print) 1532-2432 (Online) Journal homepage: http://www.tandfonline.com/loi/lsyc20
Improved Preparation of 24-Crown-8
Vladimir S. Talanov & Richard A. Bartsch
To cite this article: Vladimir S. Talanov & Richard A. Bartsch (1999) Improved Preparation of 24-
Crown-8, Synthetic Communications, 29:20, 3555-3560, DOI: 10.1080/00397919908085989
To link to this article: http://dx.doi.org/10.1080/00397919908085989
Published online: 17 Sep 2007.
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Date: 05 June 2016, At: 03:30