Journal of Fluorine Chemistry p. 557 - 570 (1987)
Update date:2022-08-10
Topics:
Wasser, D. J.
Johnson, P. S.
Klink, F. W.
Kucera, F.
Liu, Chung-Chiun
The electrochemical fluorination of acetyl fluoride in anhydrous hydrogen fluoride to produce trifluoroacetyl fluoride was investigated in a microprocessor-aided modified Simons' reactor.The product was recorvered in acetic as trifluoroacetic acid.The experiments were carried out at a controlled anodic potential using a Cu/CuF2 reference electrode.Product yields of 36-45percent, current efficiencies of 30 to 50percent and energy efficiencies of 11-23percent were obtained.Experimental results of this investigation are presented and discussed.
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Doi:10.1039/P19830002119
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