Journal of Fluorine Chemistry p. 557 - 570 (1987)
Update date:2022-08-10
Topics:
Wasser, D. J.
Johnson, P. S.
Klink, F. W.
Kucera, F.
Liu, Chung-Chiun
The electrochemical fluorination of acetyl fluoride in anhydrous hydrogen fluoride to produce trifluoroacetyl fluoride was investigated in a microprocessor-aided modified Simons' reactor.The product was recorvered in acetic as trifluoroacetic acid.The experiments were carried out at a controlled anodic potential using a Cu/CuF2 reference electrode.Product yields of 36-45percent, current efficiencies of 30 to 50percent and energy efficiencies of 11-23percent were obtained.Experimental results of this investigation are presented and discussed.
View More
Suzhou Chiral Pharmaceuticals Co., Ltd.
Contact:86-0512-63197058
Address:Building A, No. 2358, Chang'an Road, Wujiang Science Park
Beijing Apis Biotechnology Co., Ltd.
Contact:86-010-67856775-8551
Address:NO.4PUHUANGYU ROAD,FENTAI DISTRICT, BEIJING, CHINA
Shenyang Xinyihan Chemical Technology Co., Ltd.
Contact:+86-18525026267
Address:362, aigongbeijei street 23 , tiexi district,Shenyang, Liaoning, China
Chengdu Yunyi International Trade Co., Ltd
Contact:0411-39894967
Address:china
Refine Chemicals Science & Technology Technology Developing Co., Ltd.
Contact:+86-22-87899130
Address:No.12,west keyan road,Tianjin City
Doi:10.1039/P19830002119
(1983)Doi:10.1039/c4ra11411f
(2014)Doi:10.1016/j.tet.2008.07.076
(2008)Doi:10.1016/S0031-9422(00)83047-2
(1985)Doi:10.1149/1.1595662
(2003)Doi:10.1016/0022-328X(85)87318-6
(1985)
