Journal of Fluorine Chemistry p. 409 - 420 (1987)
Update date:2022-08-11
Topics:
Malik, A. A.
Sharts, C. M.
Shellhamer, D. F.
Base-catalyzed addition of simple sterols to perfluoroalkenes, to give a variety of perfluoroalkenyl steroidal ethers, has been investigated.The outcome of the reaction was dependent on the base used for deprotonation of sterols.With potassium hydride, a mixture of 1- and 2-perfluoroalkenyl steroidal ethers was obtained in a low yield, whereas with n-butyllithium, preferential formation of 1-perfluoroalkenyl steroidal ethers was achieved in high yields.
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