Bulletin of the Chemical Society of Japan p. 767 - 768 (1985)
Update date:2022-08-10
Topics:
Naemura, Koichiro
Ebashi, Iwao
Nakazaki, Masao
trans,trans-2,2'-Spirobiindan-1,1'-diol (1) was resolved as its (-)-ω-camphanic ester and the absolute rotation of the glycol 1 was determined.Two crown ethers and the acyclic analog were derived from (+)-1.Two crown ethers incorporating (+)-cis,trans-2,2'-spirobiindan-1,1'-diol were also prepared.Their chiral recognition properties in transport of methyl (+/-)phenylglycinate hydrochloride and abilities to extract alkali metal picrates were investigated.
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