Efficient Synthesis of α-Hydroxy-β-ketoesters from Methyl Phenylglyoxalate and Acid Chlorides mediated by Titanium Trichloride

DOI: 10.1016/S0040-4039(00)76800-6

Source and publish data:

Tetrahedron Letters p. 2213 - 2216 (1994)

Update date:2022-08-11

Topics:

Authors:

Araneo, Silvia

Clerici, Angelo

Porta, Ombretta

Read Full Text PDF DownLoad Join now for total 90,000,000 free articles

Article abstract of DOI:10.1016/S0040-4039(00)76800-6

Methyl phenylglyoxalate and acid chlorides undergo rapid condensation reactions on treatment with a TiCl3-THF/CH2Cl2 solution, in the presence of pyridine, at room temperature.

Full text of DOI:10.1016/S0040-4039(00)76800-6

Products guided by the article

Product name:Methyl DL-mandelate

Cas No:4358-87-6

R&D Labs maybe for 4358-87-6

Chongqing Yawei Fine Chemical Co.,Ltd

Contact:0086-23-62849407

Address:Ziyou village, Nanquan town, Banan district, Chongqing China
Shanghai ZaiQi Bio-Tech Co., Ltd.,

Contact:+86-21-5482 4098

Address:Bldg. No.7, No.201 MinYi Rd，Songjiang CaoHeJing High-Tech Park Shanghai 201516 P,R,China
Shanghai Intime pharm Co.,Ltd

Contact:86-21-58226973

Address:No 351,Guoshoujing Road, Zhangjiang Hi-tech Park, Pudong, Shanghai, China
Fuxin Jintelai Fluorin Chemical Co., Ltd.

Contact:+86-0418-8229599

Address:, 7th Huagong Road, Fluorine industry development zone (Yimatu Town,Fumeng County),Fuxin City, Liaoning Province, China
Accendatech Co., LTD

Contact:+86-22-83718541

Address:32th Floor, Rongqiao Center Intersection of Changjiang Road and Nankai Six Road Nankai District Tianjin 300102, China

Relevant to this article

Visible Light-Mediated Direct Decarboxylative C-H Functionalization of Heteroarenes

Doi:10.1021/acscatal.7b01133
(2017)
Rhodamine B degradation and reactive oxygen species generation by a ZnSe-graphene/TiO₂ sonocatalyst

Doi:10.1016/S1872-2067(14)60158-3
(2014)
Doi:10.1021/jo01060a001
(1961)
Aldol Reactions of Biorenewable Triacetic Acid Lactone Precursor Evaluated Using Desorption Electrospray Ionization Mass Spectrometry High-Throughput Experimentation and Validated by Continuous Flow Synthesis

Doi:10.1021/acscombsci.0c00119
(2020)
Immobilized hydroxynitrile lyases for enantioselective synthesis of cyanohydrins: Sol-gels and cross-linked enzyme aggregates

Doi:10.1002/adsc.200606139
(2006)
Doi:10.1039/JR9580004245
(1958)

Article Doi