Efficient Synthesis of α-Hydroxy-β-ketoesters from Methyl Phenylglyoxalate and Acid Chlorides mediated by Titanium Trichloride

DOI: 10.1016/S0040-4039(00)76800-6

Source and publish data:

Tetrahedron Letters p. 2213 - 2216 (1994)

Update date:2022-08-11

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Authors:

Araneo, Silvia

Clerici, Angelo

Porta, Ombretta

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Article abstract of DOI:10.1016/S0040-4039(00)76800-6

Methyl phenylglyoxalate and acid chlorides undergo rapid condensation reactions on treatment with a TiCl3-THF/CH2Cl2 solution, in the presence of pyridine, at room temperature.

Full text of DOI:10.1016/S0040-4039(00)76800-6

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