Journal of the Chemical Society. Perkin transactions II p. 1071 - 1074 (1983)
Update date:2022-08-11
Topics:
Lee, Kheng H.
Brumby, Steven
Free radicals formed during the photolysis of solutions containing di-t-butyl peroxide and fluoro-acetals such as 1,1-diethoxy-2-fluoroethane and substituted 1,3-dioxolanes, have been studied by e.s.r. spectroscopy.Only the radicals formed initially by hydrogen abstraction were detected, although product analysis by g.c.-m.s. indicated that certain of the cyclic radicals rearranged to acyclic species.The e.s.r. parameters are discussed in relation to the preferred conformations of the radicals.
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