A facile synthesis of per-O-alkylated glycono-δ-lactones from per-O-alkylated glycopyranosides and a novel ring contraction for pyranoses

DOI: 10.1016/S0040-4020(97)00068-9

Source and publish data:

Tetrahedron p. 3123 - 3134 (1997)

Update date:2022-08-16

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Authors:

Goebel, Matthias

Nothofer, Heinz-Georg

Ross, Guenther

Ugi, Ivar

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Article abstract of DOI:10.1016/S0040-4020(97)00068-9

A novel one-pot synthesis of a variety of O-peralkylated δ-aldonolactones 9 from their corresponding glycosides 1 is introduced. This facile procedure involves combining glycoside precursor, tin(IV) chloride and trimethylsilyl azide in methylene chloride

Full text of DOI:10.1016/S0040-4020(97)00068-9

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