Chemistry Letters p. 1097 - 1100 (1993)
Update date:2022-08-28
Topics:
Taguchi, Yoichi
Yasumoto, Masahiko
Tsuchiya, Tohru
Oishi, Akihiro
Shibuya, Isao
5,6-Dihydro-1,3,5-trimethyl-6-methylimino-1,3,5-triazine-2,4-(1H,3H)-dithione (1) was synthesized by the reaction of methyl isothiocyanate under high pressure in the presence of Et3N and H2O.The yield and selectivity of 1 were seriously effected by pressure, reaction temperature, solvent, and the amount of H2O.
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