Tetrahedron Letters p. 5389 - 5392 (1986)
Update date:2022-08-16
Topics:
Hori, Yoji
Mitsudo, Take-aki
Watanabe, Yoshihisa
Propargyl carbonates react with acetic acid in the presence of a catalytic amount of bis(η5-cyclooctadienyl)ruthenium/PCy3/maleic anhydride at 80 deg C to give 2-acetoxyallyl carbonates in good yields with excellent regioselectivity.These 2-acetoxyallyl carbonates catalytically react with carbonucleophiles in the presence of tetrakis(triphenylphosphine)palladium to give 2-acetoxyallylated products in good to excellent yields.
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