Journal of the Chemical Society. Perkin transactions I p. 3115 - 3118 (1994)
Update date:2022-08-17
Topics:
Briscoe, Mark W.
Chambers, Richard D.
Mullins, Steven J.
Nakamura, Takayuki
Vaughan, Julian F. S.
Drakesmith, Frederick G.
The oligomers 2, 4 and 6, 6a, derived from tetrafluoroethene, octafluorocyclopentene, and hexafluorocyclobutene respectively, are converted into their corresponding dienes 7-9 by defluorination, using sodium amalgam.An alternative route using tetrakis(dimethylamino)ethene (TDAE) is also described and forms a fluoride salt of TDAE.The diene 7 shows a remarkably low extinction coefficient for UV absorption.
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