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Cas Database

Name	PROPIONANILIDE	EINECS	N/A
CAS No.	620-71-3	Density	1.073g/cm³
PSA	29.10000	LogP	2.10810
Solubility	Insoluble in water.	Melting Point	104-107℃
Formula	C9H11 N O	Boiling Point	314.4°C at 760 mmHg
Molecular Weight	149.192	Flash Point	182°C
Transport Information	N/A	Appearance	N/A
Safety	Moderately toxic by ingestion. When heated to decomposition it emits toxic fumes of NO_x.	Risk Codes	N/A
Molecular Structure		Hazard Symbols	N/A
Synonyms	Propionanilide(6CI,7CI,8CI); N-Phenylpropanamide; N-Phenylpropionamide; NSC 58952; R 50977	Article Data	237

PROPIONANILIDE Synthetic route

: 23517-42-2
propiophenone oxime

: 620-71-3
N-(phenyl)-2-methylacetamide

Conditions

Conditions	Yield
With sulfuric acid; 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate for 0.0166667h; Beckmann rearrangement; microwave irradiation;	100%
mercury dichloride In acetonitrile at 80℃; for 8h; Beckmann rearrangement;	98%
With bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; zinc(II) chloride In acetonitrile for 1h; Beckmann rearrangement; Heating;	97%

: 2157-50-8
propiophenone oxime

: 620-71-3
N-(phenyl)-2-methylacetamide

Conditions

Conditions	Yield
With 1,1'-carbonyldiimidazole; methyl iodide In acetonitrile for 1h; Heating;	98%
With p-toluenesulfonyl chloride; zinc(II) chloride In acetonitrile for 1h; Beckmann rearrangement; Inert atmosphere; Reflux;	98%
With silica gel; caesium carbonate; N-tosylimidazole In N,N-dimethyl-formamide for 2h; Beckmann rearrangement; Reflux;	98%

: 802294-64-0
propionic acid

: 62-53-3
aniline

: 620-71-3
N-(phenyl)-2-methylacetamide

Conditions

Conditions	Yield
With fluorosulfonyl fluoride; N-ethyl-N,N-diisopropylamine In acetonitrile at 20℃; for 5h;	98%
Stage #1: propionic acid With iodine; triethylamine; phosphorous acid trimethyl ester In dichloromethane for 0.166667h; Cooling with ice; Inert atmosphere; Stage #2: aniline In dichloromethane at 20℃; for 3h; Inert atmosphere; Cooling with ice;	96%
With [((CH3)5Cp)2Zr(H2O)2OSO2C8F17]+[OSO2C8F17]-*THF In neat (no solvent) at 80℃; for 2h;	94%

: 74-85-1
ethene

: 201230-82-2
carbon monoxide

: 62-53-3
aniline

: 620-71-3
N-(phenyl)-2-methylacetamide

Conditions

Conditions	Yield
With palladium(II) acetylacetonate In toluene at 100℃; under 30003 Torr; for 20h; Autoclave; Inert atmosphere; regioselective reaction;	98%
With C52H52NO5P; palladium(II) iodide In tetrahydrofuran at 60℃; under 760.051 Torr; for 72h; Autoclave; regioselective reaction;	93%
With Ru-clusters supported on ceria In tetrahydrofuran at 160℃; under 7500.75 Torr; for 24h; Autoclave;	67%
Co/C In water at 150℃; under 53203.6 Torr; for 72h;	54%

: 369-57-3
benzenediazonium tetrafluoroborate

: 107-12-0
propiononitrile

: 620-71-3
N-(phenyl)-2-methylacetamide

Conditions

Conditions	Yield
Stage #1: benzenediazonium tetrafluoroborate; propiononitrile for 0.0166667h; Microwave irradiation; Stage #2: With water In diethyl ether	97%

: 71-23-8
propan-1-ol

: 62-53-3
aniline

: 620-71-3
N-(phenyl)-2-methylacetamide

Conditions

Conditions	Yield
With oxygen; sodium hydroxide In water at 40℃; for 24h;	97%
With oxygen; sodium hydroxide In water at 40℃; for 24h; Green chemistry;	94%
With potassium tert-butylate In 1,4-dioxane at 110℃; for 24h;	88%

: 123-62-6
propionic acid anhydride

: 62-53-3
aniline

: 620-71-3
N-(phenyl)-2-methylacetamide

Conditions

Conditions	Yield
With tris(pentafluorophenyl)borate In neat (no solvent) at 20℃; for 0.0333333h; Green chemistry;	96%
With sodium dodecyl-sulfate In water	87%

: 93-55-0
1-phenyl-propan-1-one

: 620-71-3
N-(phenyl)-2-methylacetamide

Conditions

Conditions	Yield
With trifluorormethanesulfonic acid; hydroxylamine hydrochloride In formic acid for 7h; Heating;	96%
With sodium azide; sulfuric acid; silica gel at 60℃; for 0.5h; Schmidt reaction;	95%
With zinc(II) chloride; hydroxylamine-O-sulfonic acid In water at 20℃; for 16h; Beckmann Rearrangement;	93%

: 802294-64-0
propionic acid

: 622-37-7
Phenyl azide

: 620-71-3
N-(phenyl)-2-methylacetamide

Conditions

Conditions	Yield
With triphenylphosphine In benzene for 60h; Heating;	96%
With triethylphosphine In benzene at 80℃; for 12h;	87%

: 7341-97-1
N-phenyl propynamide

: 620-71-3
N-(phenyl)-2-methylacetamide

Conditions

Conditions	Yield
With hydrogen for 1h;	94%

PROPIONANILIDE Chemical Properties

Propionanilide is also named as n-phenyl-propanamid;N-Phenylpropanamide;Propionamide, N-phenyl-;Propionic anilide,and so on.

Molecular Formula: C₉H₁₁NO
Molecular Weight: 149.19
EINECS: 210-649-3

PROPIONANILIDE Toxicity Data With Reference

Test type: LD₅₀- Lethal dose, 50 percent kill
Contact:    Oral
Species:     Rodent - mouse
Dose:        1100 mg/kg
Toxic effect:Details of toxic effects not reported other than lethal dose value
Referrence: TXAPA9 Toxicology and Applied Pharmacology. (Academic Press, Inc., 1 E. First St., Duluth, MN 55802) V.1- 1959- Volume(issue)/page/year: 19,20,1971

RTECS:UE4600000

PROPIONANILIDE Consensus Reports

Reported in EPA TSCA Inventory.

EPA TSCA Section 8(b) CHEMICAL INVENTORY EPA TSCA TEST SUBMISSION (TSCATS) DATA BASE, JUNE 1998

PROPIONANILIDE Safety Profile

Propionanilide is moderately toxic by ingestion. When heated to decomposition it emits toxic fumes of NO_x.

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