Benzaldehyde, 3-chloro-4,5-bis(phenylmethoxy)-

Base Information

Chemical Name:Benzaldehyde, 3-chloro-4,5-bis(phenylmethoxy)-
CAS No.:33584-87-1
Molecular Formula:C21H17ClO3
Molecular Weight:352.81100
Hs Code.:

Synonyms:3,4-dibenzyloxy-5-chlorobenzaldehyde;3,4-Dibenzyloxy-5-chlor-benzaldehyd;5-chloro-3,4-dibenzyloxybenzaldehyde;5-Chlor-3,4-dibenzyloxybenzaldehyd;

Suppliers and Price of Benzaldehyde, 3-chloro-4,5-bis(phenylmethoxy)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzaldehyde, 3-chloro-4,5-bis(phenylmethoxy)-

Chemical Property:

PSA：35.53000
LogP:5.31050

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzaldehyde, 3-chloro-4,5-bis(phenylmethoxy)-

There total 5 articles about Benzaldehyde, 3-chloro-4,5-bis(phenylmethoxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 34098-18-5
5-chloro-3,4-dihydroxybenzaldehyde

: 100-39-0
benzyl bromide

: 33584-87-1
3-chloro-4,5-di(phenylmethoxy)benzaldehyde

Guidance literature:: With potassium carbonate; potassium iodide; In acetone; for 25h; Heating;
DOI:10.1021/jo0491399

Reference yield:

: 19463-48-0
5-chlorovanillin

: 33584-87-1
3-chloro-4,5-di(phenylmethoxy)benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / boron tribromide / CH₂Cl₂ / 4.3 h / 0 - 25 °C

2: 78 percent / KI; K₂CO₃ / acetone / 25 h / Heating

With boron tribromide; potassium carbonate; potassium iodide; In dichloromethane; acetone;
DOI:10.1021/jo0491399

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 33584-87-1
3-chloro-4,5-di(phenylmethoxy)benzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / chlorine / acetic acid / 0.5 h / 25 °C

2: 94 percent / boron tribromide / CH₂Cl₂ / 4.3 h / 0 - 25 °C

3: 78 percent / KI; K₂CO₃ / acetone / 25 h / Heating

With chlorine; boron tribromide; potassium carbonate; potassium iodide; In dichloromethane; acetic acid; acetone;
DOI:10.1021/jo0491399