4-CHLORO-4'-METHOXYBENZHYDROL

Base Information

• Chemical Name: 4-CHLORO-4'-METHOXYBENZHYDROL
• CAS No.: 34979-37-8
• Molecular Formula: C14H13ClO2
• Molecular Weight: 248.709
• Hs Code.: 2909499000
• Mol file: 34979-37-8.mol

Synonyms:4-chloro-4'metoxydiphenylmethanol;4-chloro-4'-methoxybenzhydrol;4-chloro-4'-methoxy-benzhydrol;(p-anisyl)(4-chlorophenyl)methanol;(+/-)-Hydroxy-(4-chlor-phenyl)-(4-methoxy-phenyl)-methan;4-chlorophenyl(4-methoxyphenyl)methanol;

Chemical Property of 4-CHLORO-4'-METHOXYBENZHYDROL

Chemical Property:

• PSA: 29.46000
• LogP: 3.43030

Purity/Quality:

99% ^*data from raw suppliers

(4-CHLOROPHENYL)(4-METHOXYPHENYL)METHANOL ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-CHLORO-4'-METHOXYBENZHYDROL

There total 10 articles about 4-CHLORO-4'-METHOXYBENZHYDROL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

4-methoxyphenylboronic acid (5720-07-0) + 4-chlorobenzaldehyde (104-88-1) → (4-chlorophenyl)(4-methoxyphenyl)methanol (34979-37-8)

Guidance literature:

With potassium tert-butylate; In 1,4-dioxane; water; at 80 ℃; for 6h;

DOI:10.1039/c1cc14898b

Reference yield: 95.0%

1-Chloro-4-iodobenzene (637-87-6) + 4-methoxy-benzaldehyde (123-11-5) → (4-chlorophenyl)(4-methoxyphenyl)methanol (34979-37-8)

Guidance literature:

With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 2.77778E-05h; Flow reactor;

DOI:10.1055/s-0040-1707259

Reference yield: 81.0%

4-chlorobenzaldehyde (104-88-1) + 4-methoxyphenyl magnesium bromide (13139-86-1) → (4-chlorophenyl)(4-methoxyphenyl)methanol (34979-37-8)

Guidance literature:

In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/acs.joc.5b02273

upstream raw materials:

4-chloro-4'-methoxybenzophenone

C₁₄H₁₂ClO⁽¹⁺⁾

4-chlorobenzaldehyde

4-methoxyphenyl magnesium bromide

Downstream raw materials:

{2-[(4-Chloro-phenyl)-(4-methoxy-phenyl)-methoxy]-ethyl}-dimethyl-amine

4-chloro-4'-methoxybenzophenone

C₂₃H₂₉ClO₃

C₂₁H₁₆Cl₂O₃

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