2-Methyleneoctanoic acid methyl ester

Base Information

Chemical Name:2-Methyleneoctanoic acid methyl ester
CAS No.:3618-40-4
Molecular Formula:C10H18O2
Molecular Weight:170.252
Hs Code.:2916190090
Mol file:3618-40-4.mol

Synonyms:2-Hexyl-acrylsaeure-methylester;Methyl 2-hexyl acrylate;2-hexyl-acrylic acid methyl ester;Methyl 2-methyleneoctanoate;Octanoic acid,2-methylene-,methyl ester;

Suppliers and Price of 2-Methyleneoctanoic acid methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
methyl2-methylideneoctanoate
10mg
$ 65.00

Total 5 raw suppliers

Chemical Property of 2-Methyleneoctanoic acid methyl ester

Chemical Property:

PSA：26.30000
LogP:2.68600

Purity/Quality:

95% ^*data from raw suppliers

methyl2-methylideneoctanoate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-Methyleneoctanoic acid methyl ester

There total 3 articles about 2-Methyleneoctanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: 629-05-0
n-octyne

: 201230-82-2
carbon monoxide

: 111-79-5
methyl 2-nonenoate

: 3618-40-4
Methyl 2-methyleneoctanoate

Guidance literature:: With [Pd₂(H₂O)4(dppcb)](OTs)4; hydrogen; In acetonitrile; at 70 ℃; for 2h; under 7757.43 Torr; regioselective reaction; Autoclave; Inert atmosphere;
DOI:10.1021/om3003812

Reference yield:

: 629-05-0
n-octyne

: 124-38-9,18923-20-1
carbon dioxide

: 74-88-4
methyl iodide

: 111-79-5
methyl 2-nonenoate

: 3618-40-4
Methyl 2-methyleneoctanoate

Guidance literature:: With tris(2,2'-bipyridine)nickel(II) tetrafluoroborate; tetrabutylammonium tetrafluoroborate; potassium carbonate; magnesium; Yield given. Multistep reaction. Yields of byproduct given; 1.) one-compartment cell electrosynthesis, DMF, 20 deg C, 7 h, 2.) DMF, 50 deg C, 5 h;
DOI:10.1021/ja00022a037

Reference yield:

: 67-56-1
methanol

: 629-05-0
n-octyne

: 201230-82-2
carbon monoxide

: 14952-06-8
methyl (2E)-2-nonenoate

: 3618-40-4
Methyl 2-methyleneoctanoate

Guidance literature:: With dichloro bis(acetonitrile) palladium(II); 1-(2,5-bis(diphenylphosphanyl)thiophen-3'-yl)-2-(diphenylphosphanyl)-3-methyl-1H-imidazol-3-ium trifluoromethanesulfonate; In water; toluene; at 110 ℃; for 8h; under 22502.3 Torr; Autoclave;
DOI:10.1016/j.jcat.2019.01.031