N,N,2-Trimethylbut-2-en-1-amine

Base Information

• Chemical Name: N,N,2-Trimethylbut-2-en-1-amine
• CAS No.: 40267-41-2
• Molecular Formula: C7H15N
• Molecular Weight: 113.203
• DSSTox Substance ID: DTXSID40707142
• Mol file: 40267-41-2.mol

Synonyms:N,N,2-Trimethylbut-2-en-1-amine;40267-41-2;SCHEMBL15901680;DTXSID40707142

Chemical Property of N,N,2-Trimethylbut-2-en-1-amine

Chemical Property:

• XLogP3: 1.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 113.120449483
• Heavy Atom Count: 8
• Complexity: 82.4

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC=C(C)CN(C)C

Technology Process of N,N,2-Trimethylbut-2-en-1-amine

There total 3 articles about N,N,2-Trimethylbut-2-en-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

DIMCARB (4137-10-4) + isoprene (78-79-5,9003-31-0) → prenyldimethylamine (2588-79-6) + 1-Dimethylamino-2-methyl-2-butene (40267-41-2)

Guidance literature:

With sodium 1,4-bis[(di-m-sulfonatophenyl)phosphino]butane; palladium(II) trifluoroacetate; In neat (no solvent); at 100 ℃; for 3h; Overall yield = 93 %Chromat.; Catalytic behavior;

DOI:10.1039/c7gc02272g

Reference yield:

dimethyl amine (124-40-3) + acrylonitrile (107-13-1,25014-41-9) + isoprene (78-79-5,9003-31-0) → 1-Dimethylamino-2-methyl-2-butene (40267-41-2) + N-(1,1-dimethyl-3-dimethylaminopropyl)-acrylamide (34730-67-1)

Guidance literature:

With sulfuric acid; hydroquinone; Yield given. Multistep reaction. Yields of byproduct given; 2.) 2.5 h, 62 deg C;

Reference yield:

dimethyl amine (124-40-3) + acrylonitrile (107-13-1,25014-41-9) + isoprene (78-79-5,9003-31-0) → 1-Dimethylamino-2-methyl-2-butene (40267-41-2) + N-(1,1-dimethyl-3-dimethylaminopropyl)-acrylamide (34730-67-1) + dimethyl-(3-methyl-but-1-enyl)-amine (18495-55-1)

Guidance literature:

With sulfuric acid; sodium; hydroquinone; Multistep reaction. Yields of byproduct given; 1.) 25 deg C, 2 h;

upstream raw materials:

dimethyl amine

acrylonitrile

isoprene

DIMCARB