N-[4-(dimethylamino)-2-methylbutan-2-yl]prop-2-enamide

Base Information

• Chemical Name: N-[4-(dimethylamino)-2-methylbutan-2-yl]prop-2-enamide
• CAS No.: 34730-67-1
• Molecular Formula: C10H20N2O
• Molecular Weight: 184.27900
• DSSTox Substance ID: DTXSID20364671
• Nikkaji Number: J728.235D
• Wikidata: Q82148750
• Mol file: 34730-67-1.mol

Synonyms:34730-67-1;N-(1,1-dimethyl-3-dimethylaminopropyl)acrylamide;N-[4-(dimethylamino)-2-methylbutan-2-yl]prop-2-enamide;SCHEMBL1018029;DTXSID20364671;STL563276;3-Acrylamido-3-methylbutyldimethylamin;AKOS000601923;N-[1,1-Dimethyl-3-(dimethylamino)propyl]acrylamide

Chemical Property of N-[4-(dimethylamino)-2-methylbutan-2-yl]prop-2-enamide

Chemical Property:

• Vapor Pressure: 0.000813mmHg at 25°C
• Boiling Point: 305.6oC at 760 mmHg
• Flash Point: 138.6oC
• PSA: 35.83000
• Density: 0.912g/cm3
• LogP: 1.85920
• XLogP3: 1.1
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 5
• Exact Mass: 184.157563266
• Heavy Atom Count: 13
• Complexity: 185

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C)(CCN(C)C)NC(=O)C=C

Technology Process of N-[4-(dimethylamino)-2-methylbutan-2-yl]prop-2-enamide

There total 3 articles about N-[4-(dimethylamino)-2-methylbutan-2-yl]prop-2-enamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dimethyl amine (124-40-3) + acrylonitrile (107-13-1,25014-41-9) + isoprene (78-79-5,9003-31-0) → 1-Dimethylamino-2-methyl-2-butene (40267-41-2) + N-(1,1-dimethyl-3-dimethylaminopropyl)-acrylamide (34730-67-1)

Guidance literature:

With sulfuric acid; hydroquinone; Yield given. Multistep reaction. Yields of byproduct given; 2.) 2.5 h, 62 deg C;

Reference yield:

dimethyl amine (124-40-3) + acrylonitrile (107-13-1,25014-41-9) + isoprene (78-79-5,9003-31-0) → 1-Dimethylamino-2-methyl-2-butene (40267-41-2) + N-(1,1-dimethyl-3-dimethylaminopropyl)-acrylamide (34730-67-1) + dimethyl-(3-methyl-but-1-enyl)-amine (18495-55-1)

Guidance literature:

With sulfuric acid; sodium; hydroquinone; Multistep reaction. Yields of byproduct given; 1.) 25 deg C, 2 h;

Reference yield:

→ N-(1,1-dimethyl-3-dimethylaminopropyl)-acrylamide (34730-67-1)

Guidance literature:

upstream raw materials:

dimethyl amine

acrylonitrile

isoprene

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