5-CHLORO-N,N-DIMETHYL-2-NITRO-BENZAMIDE

Base Information

• Chemical Name: 5-CHLORO-N,N-DIMETHYL-2-NITRO-BENZAMIDE
• CAS No.: 480451-75-0
• Molecular Formula: C9H9ClN2O3
• Molecular Weight: 228.635
• Hs Code.: 2924299090
• Mol file: 480451-75-0.mol

Synonyms:5-Chlor-2-nitro-benzoesaeure-dimethylamid;5-chloro-2-nitro-benzoic acid dimethylamide;

Chemical Property of 5-CHLORO-N,N-DIMETHYL-2-NITRO-BENZAMIDE

Chemical Property:

• Vapor Pressure: 1.38E-06mmHg at 25°C
• Boiling Point: 399.4oC at 760 mmHg
• Flash Point: 195.3oC
• PSA: 66.13000
• Density: 1.356g/cm3
• LogP: 2.47320
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

5-Chloro-N,N-dimethyl-2-nitrobenzamide 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-CHLORO-N,N-DIMETHYL-2-NITRO-BENZAMIDE

There total 5 articles about 5-CHLORO-N,N-DIMETHYL-2-NITRO-BENZAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C10H6ClN3O3 + N,N-dimethylammonium chloride (506-59-2) → 5-chloro-N,N-dimethyl-2-nitrobenzamide (480451-75-0)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 20 ℃; Reflux;

Reference yield:

5-chloro-2-nitrobenzoyl chloride (41994-44-9) + dimethyl amine (124-40-3) → 5-chloro-N,N-dimethyl-2-nitrobenzamide (480451-75-0)

Guidance literature:

With diethyl ether;

Reference yield:

5-chloro-2-nitrobenzoic acid (2516-95-2) + N,N-dimethylammonium chloride (506-59-2) → 5-chloro-N,N-dimethyl-2-nitrobenzamide (480451-75-0)

Guidance literature:

With 1-ethyl-3-(3-dimethylaminopyridyl)carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine; In N,N-dimethyl-formamide;

upstream raw materials:

5-chloro-2-nitrobenzoyl chloride

dimethyl amine

5-chloro-2-nitrobenzoic acid

N,N-dimethylammonium chloride

Downstream raw materials:

2-amino-5-chloro-N,N-dimethyl-benzamide

1-(3-Dimethylcarbamoyl-4-nitrophenyl)piperidine-4-carboxylic acid ethyl ester

5-benzyloxy-N,N-dimethyl-2-nitrobenzamide

(3-dimethylcarbamoyl-4-nitrophenyl)acetic acid methyl ester