1,2-Dichlorocyclohexane

Base Information

• Chemical Name: 1,2-Dichlorocyclohexane
• CAS No.: 1121-21-7
• Molecular Formula: C6H10 Cl2
• Molecular Weight: 153.051
• Hs Code.: 2903890090
• Mol file: 1121-21-7.mol

Synonyms:1,2-Dichlorocyclohexane;NSC 97192

Chemical Property of 1,2-Dichlorocyclohexane

Chemical Property:

• Boiling Point: 198°Cat760mmHg
• Flash Point: 66.1°C
• PSA: 0.00000
• Density: 1.14g/cm³
• LogP: 2.77520

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,2-Dichlorocyclohexane

There total 42 articles about 1,2-Dichlorocyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

cyclohexane-1,2-epoxide (286-20-4) → 1,2-dichlorocyclohexane (1121-21-7)

Guidance literature:

With N-chloro-succinimide; [(PhNH)P₂(NPh)2]2NPh; In acetonitrile; for 4h; Reflux;

DOI:10.1080/10426507.2014.906420

Reference yield: 34.0%

cyclohexene (110-83-8) → bicyclohexyl-2,2'-diene (1541-20-4) + 1,2-dichlorocyclohexane (1121-21-7) + 2-chlorocyclohexanol (1561-86-0) + cyclohexane-1,2-epoxide (286-20-4) + cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) + Cyclohex-2-enol (822-67-3)

Guidance literature:

With potassium hexachloropalatinate(IV); dihydroxo[tetraphenylporphyrinato]antimony(V) hexafluorophosphate; water; In acetonitrile; for 1h; Product distribution; Mechanism; Irradiation; various reaction conditions;

DOI:10.1021/ja971371r

Reference yield: 28.0%

C6H4Cl4Te → 1,2-dichlorocyclohexane (1121-21-7)

Guidance literature:

In benzene; at 20 - 25 ℃; Irradiation;

DOI:10.1246/cl.1980.943

upstream raw materials:

N-chloro-succinimide

cyclohexene

tetrachloromethane

thiophene

Downstream raw materials:

cyclohexene

1,2-cyclohexane dicarboxylic acid di-isononylester

hexabromobenzene

1,2-diphenyl-cyclohexane