5-(Methylthio)benzo[d][1,3]dioxole

Base Information

Chemical Name:5-(Methylthio)benzo[d][1,3]dioxole
CAS No.:5354-08-5
Molecular Formula:C8H8O2S
Molecular Weight:168.216
Hs Code.:2932999099
DSSTox Substance ID:DTXSID70517892
Nikkaji Number:J3.235.292H
Wikidata:Q82380158
Mol file:5354-08-5.mol

Synonyms:5-(Methylthio)benzo[d][1,3]dioxole;5354-08-5;5-methylsulfanyl-1,3-benzodioxole;3,4-(Methylenedioxy)phenyl methyl sulfide;SCHEMBL3464473;DTXSID70517892;BUKOTIQMZLCUGO-UHFFFAOYSA-N;5-(methylthio)-1,3-benzodioxole;AKOS006315546;5-(Methylsulfanyl)-2H-1,3-benzodioxole

Suppliers and Price of 5-(Methylthio)benzo[d][1,3]dioxole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Chemenu
5-(methylthio)benzo[d][1,3]dioxole 95%
1g
$ 356.00

American Custom Chemicals Corporation
5-(METHYLTHIO)BENZO[D][1,3]DIOXOLE 95.00%
5MG
$ 497.92

Alichem
5-(Methylthio)benzo[d][1,3]dioxole
1g
$ 400.00

Total 6 raw suppliers

Chemical Property of 5-(Methylthio)benzo[d][1,3]dioxole

Chemical Property:

PSA：43.76000
LogP:2.13720
Storage Temp.:2-8°C
XLogP3:2.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:168.02450067
Heavy Atom Count:11
Complexity:140

Purity/Quality:

95% ^*data from raw suppliers

5-(methylthio)benzo[d][1,3]dioxole 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CSC1=CC2=C(C=C1)OCO2

Technology Process of 5-(Methylthio)benzo[d][1,3]dioxole

There total 6 articles about 5-(Methylthio)benzo[d][1,3]dioxole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 2635-13-4
1,2-(methylenedioxy)-4-bromobenzene

: 624-92-0
Dimethyldisulphide

: 5354-08-5
5-(methylthio)benzo[d][1,3]dioxole

Guidance literature:: 1,2-(methylenedioxy)-4-bromobenzene; With n-butyllithium; In tetrahydrofuran; hexanes; at -78 ℃; for 0.5h;

Dimethyldisulphide; In tetrahydrofuran; hexanes; for 0.5h;

Reference yield: 78.0%

: 6698-13-1
4-bromo-benzo[1,3]dioxole

: 67-68-5,8070-53-9
dimethyl sulfoxide

: 5354-08-5
5-(methylthio)benzo[d][1,3]dioxole

Guidance literature:: With copper(l) iodide; zinc diacetate; at 135 ℃; for 36h; regioselective reaction;
DOI:10.1016/j.tet.2013.07.039

Reference yield: 59.0%

: 5271-38-5
2-methylmercapto-ethanol

: 5876-51-7
5-iodo-1,3-benzodioxole

: 5354-08-5
5-(methylthio)benzo[d][1,3]dioxole

Guidance literature:: With potassium tert-butylate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; palladium dichloride; In 5,5-dimethyl-1,3-cyclohexadiene; at 120 ℃; for 12h;
DOI:10.1039/c9sc05532k