1-(5-Chloro-2-methylphenyl)ethanone

Base Information

Chemical Name:1-(5-Chloro-2-methylphenyl)ethanone
CAS No.:58966-35-1
Molecular Formula:C9H9ClO
Molecular Weight:168.623
Hs Code.:2914700090
DSSTox Substance ID:DTXSID10570603
Wikidata:Q82458110
Mol file:58966-35-1.mol

Synonyms:1-(5-Chloro-2-methylphenyl)ethanone;58966-35-1;1-(5-chloro-2-Methylphenyl)ethan-1-one;Ethanone, 1-(5-chloro-2-methylphenyl)-;SCHEMBL3922668;DTXSID10570603;AMY19178;AKOS006307969;AS-63814;CS-0061174;F52542;EN300-2967106

Suppliers and Price of 1-(5-Chloro-2-methylphenyl)ethanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Rieke Metals
1-(5-Chloro-2-methylphenyl)ethanone
5g
$ 754.00

Rieke Metals
1-(5-Chloro-2-methylphenyl)ethanone
1g
$ 254.00

Crysdot
1-(5-Chloro-2-methylphenyl)ethanone 95+%
1g
$ 339.00

Chemcia Scientific
1-(5-Chloro-2-methyl-phenyl)-ethanone 95%
1 G
$ 225.00

Alichem
5'-Chloro-2'-methylacetophenone
1g
$ 1549.60

AK Scientific
1-(5-chloro-2-methylphenyl)ethanone
1g
$ 340.40

AHH
1-(5-chloro-2-methylphenyl)ethanone 97%
1g
$ 285.00

Total 12 raw suppliers

Chemical Property of 1-(5-Chloro-2-methylphenyl)ethanone

Chemical Property:

Boiling Point:121-122 °C(Press: 7 Torr)
PSA：17.07000
Density:1.159 g/cm3(Temp: 30 °C)
LogP:2.85100
Storage Temp.:2-8°C
XLogP3:2.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:168.0341926
Heavy Atom Count:11
Complexity:156

Purity/Quality:

97% ^*data from raw suppliers

1-(5-Chloro-2-methylphenyl)ethanone ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=C(C=C1)Cl)C(=O)C

Technology Process of 1-(5-Chloro-2-methylphenyl)ethanone

There total 5 articles about 1-(5-Chloro-2-methylphenyl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 50712-70-4
5-chloro-2-methylbenzonitrile

: 74-88-4
methyl iodide

: 58966-35-1
1-(5-chloro-2-methylphenyl)ethan-1-one

Guidance literature:: methyl iodide; With iodine; magnesium; In diethyl ether; for 0.5h; Heating / reflux;

5-chloro-2-methylbenzonitrile; In diethyl ether; at 20 ℃; Heating / reflux;

With sulfuric acid; In diethyl ether; water; at 40 ℃; for 1h;

Reference yield: 69.0%

: 50712-70-4
5-chloro-2-methylbenzonitrile

: 75-16-1
methylmagnesium bromide

: 58966-35-1
1-(5-chloro-2-methylphenyl)ethan-1-one

Guidance literature:: 5-chloro-2-methylbenzonitrile; methylmagnesium bromide; In tetrahydrofuran; at 65 ℃; for 15h;

With hydrogenchloride; water;

Reference yield:

: 27139-97-5
2-bromo-4-chloro-1-methyl-benzene

: 75-36-5
acetyl chloride

: 58966-35-1
1-(5-chloro-2-methylphenyl)ethan-1-one

Guidance literature:: 2-bromo-4-chloro-1-methyl-benzene; With magnesium; In tetrahydrofuran;

acetyl chloride; In tetrahydrofuran; at 0 - 20 ℃;