Isoquinolinium, 3,4-dihydro-2-methyl-, bromide

Base Information

Chemical Name:Isoquinolinium, 3,4-dihydro-2-methyl-, bromide
CAS No.:62753-44-0
Molecular Formula:C10H12N.Br
Molecular Weight:226.116
Hs Code.:
DSSTox Substance ID:DTXSID30487820

Synonyms:Isoquinolinium, 3,4-dihydro-2-methyl-, bromide;62753-44-0;SCHEMBL1821620;DTXSID30487820

Suppliers and Price of Isoquinolinium, 3,4-dihydro-2-methyl-, bromide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Isoquinolinium, 3,4-dihydro-2-methyl-, bromide

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:225.01531
Heavy Atom Count:12
Complexity:172

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[N+]1=CC2=CC=CC=C2CC1.[Br-]

Technology Process of Isoquinolinium, 3,4-dihydro-2-methyl-, bromide

There total 1 articles about Isoquinolinium, 3,4-dihydro-2-methyl-, bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 22901-09-3
2-(2-bromoethyl)benzaldehyde

: 74-89-5
methylamine

: 62753-44-0
2-Methyl-3,4-dihydroisoquinolinium bromide

Guidance literature:: In ethyl acetate;

Reference yield:

: 62753-44-0
2-Methyl-3,4-dihydroisoquinolinium bromide

: 100-58-3
phenylmagnesium bromide

: 7149-64-6
2-methyl-1-phenyl-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: In tetrahydrofuran; acetonitrile; at 0 ℃; Inert atmosphere; Darkness;
DOI:10.3762/bjoc.10.316

Reference yield:

: 62753-44-0
2-Methyl-3,4-dihydroisoquinolinium bromide

: 121409-51-6
2-(2-methyl-1,2,3,4-tetrahydroisoquinolin-1-yl)-1-phenylethan-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / ethanol / 0.33 h / 0 °C

2: 72 percent / 3 h / 50 - 60 °C

In ethanol;
DOI:10.1055/s-1988-27786