Silanamine, 1,1,1-trimethyl-N-(4-methylphenyl)-

Base Information

• Chemical Name: Silanamine, 1,1,1-trimethyl-N-(4-methylphenyl)-
• CAS No.: 63911-83-1
• Molecular Formula: C10H17NSi
• Molecular Weight: 179.337
• DSSTox Substance ID: DTXSID10451660
• Nikkaji Number: J282.747F
• Wikidata: Q82271782

Synonyms:N-trimethylsilyl-p-toluidine;Silanamine, 1,1,1-trimethyl-N-(4-methylphenyl)-;63911-83-1;SCHEMBL4957318;DTXSID10451660;GKOGJMSMAQANGB-UHFFFAOYSA-N;4-Methyl-N-(trimethylsilyl)benzenamine

Chemical Property of Silanamine, 1,1,1-trimethyl-N-(4-methylphenyl)-

Chemical Property:

• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 179.113026081
• Heavy Atom Count: 12
• Complexity: 131

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC=C(C=C1)N[Si](C)(C)C

Technology Process of Silanamine, 1,1,1-trimethyl-N-(4-methylphenyl)-

There total 4 articles about Silanamine, 1,1,1-trimethyl-N-(4-methylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

chloro-trimethyl-silane (75-77-4) + p-toluidine (106-49-0,12221-03-3) → 1,1,1-trimethyl-N-(4-methylphenyl)silanamine (63911-83-1)

Guidance literature:

p-toluidine; With tert.-butyl lithium; In diethyl ether; pentane; at -25 ℃; for 0.0833333h; Inert atmosphere;

chloro-trimethyl-silane; In diethyl ether; pentane; at -25 - 20 ℃; for 2h; Inert atmosphere;

DOI:10.1002/anie.201708921

Reference yield: 83.0%

p-toluidine (106-49-0,12221-03-3) + 1,1,1,3,3,3-hexamethyl-disilazane (999-97-3) → 1,1,1-trimethyl-N-(4-methylphenyl)silanamine (63911-83-1)

Guidance literature:

With saccharin; at 130 ℃; for 2h;

DOI:10.1021/jo00141a031

Reference yield:

p-toluidine (106-49-0,12221-03-3) + lithium hexamethyldisilazane (4039-32-1) → 1,1,1-trimethyl-N-(4-methylphenyl)silanamine (63911-83-1)

Guidance literature:

With ammonium chloride; for 10h; Reflux;

DOI:10.1016/j.tetlet.2012.11.090

upstream raw materials:

chloro-trimethyl-silane

p-toluidine

1,1,1,3,3,3-hexamethyl-disilazane

lithium hexamethyldisilazane

Downstream raw materials:

C₁₆H₂₁BClNSi

N-(4-methylphenylaminothio)phthalimide

3-(4-methylanilino)-3-cyclobuten-1,2-dion

4-methyl-N-<2,2,2-trifluoro-1-<5-methyl-2-(1-pyrrolidinyl)>-phenylethylidene>benzeneamine

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