6-Oxo-2,4-cyclohexadienylidenediacetate

Base Information

• Chemical Name: 6-Oxo-2,4-cyclohexadienylidenediacetate
• CAS No.: 64248-49-3
• Molecular Formula: C10H10O5
• Molecular Weight: 210.186
• Mol file: 64248-49-3.mol

Synonyms:6,6-Diacetoxy-cyclohexa-2,4-dienon;2,2-Diacetoxy-cyclohexa-3,5-dienon-1;6,6-Diacetoxy-2,4-cyclohexadienon;6,6-diacetoxy-cyclohexa-2,4-dienone;6,6-Diacetoxy-2,4-cyclohexadien-1-on;o-Chinon-diacetat;

Chemical Property of 6-Oxo-2,4-cyclohexadienylidenediacetate

Chemical Property:

• PSA: 69.67000
• LogP: 0.50400

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6-Oxo-2,4-cyclohexadienylidenediacetate

There total 6 articles about 6-Oxo-2,4-cyclohexadienylidenediacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.6%

2-acetoxyphenol (2848-25-1) → 6-oxocyclohexa-2,4-diene-1,1-diyl diacetate (64248-49-3)

Guidance literature:

With lead(IV) tetraacetate; acetic acid; In dichloromethane; at 20 ℃; Inert atmosphere;

DOI:10.1021/ja4077364

Reference yield:

lead(IV) tetraacetate (546-67-8) + 2-oxo-1,3,2-benzodioxathiolene (6255-58-9) → dimethyl phthalate (635-67-6) + 6-oxocyclohexa-2,4-diene-1,1-diyl diacetate (64248-49-3)

Guidance literature:

With pyridine; Yield given. Multistep reaction; 1.) glacial HAc, reflux, 5 h, 2.) glacial HAc, room temp., 12 h;

Reference yield:

[1-14C]phenol (22167-43-7) + phenol (108-95-2,27073-41-2) → 6-oxocyclohexa-2,4-diene-1,1-diyl diacetate (64248-49-3)

Guidance literature:

With lead(IV) acetate; In acetic acid;

DOI:10.1016/S0040-4020(01)92744-9

upstream raw materials:

2-acetoxyphenol

lead(IV) tetraacetate

acetic acid

phenol

Downstream raw materials:

pyrogallol triacetate

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