(2-Bromo-1-ethoxyethyl)benzene

Base Information

• Chemical Name: (2-Bromo-1-ethoxyethyl)benzene
• CAS No.: 6589-30-6
• Molecular Formula: C10H13BrO
• Molecular Weight: 229.117
• DSSTox Substance ID: DTXSID70505198
• Nikkaji Number: J32.107I
• Mol file: 6589-30-6.mol

Synonyms:(2-Bromo-1-ethoxyethyl)benzene;6589-30-6;SCHEMBL10986680;DTXSID70505198;alpha-(bromomethyl)benzyl ethyl ether;AKOS011393400;EN300-1133388

Chemical Property of (2-Bromo-1-ethoxyethyl)benzene

Chemical Property:

• XLogP3: 2.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 4
• Exact Mass: 228.01498
• Heavy Atom Count: 12
• Complexity: 110

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CCOC(CBr)C1=CC=CC=C1

Technology Process of (2-Bromo-1-ethoxyethyl)benzene

There total 7 articles about (2-Bromo-1-ethoxyethyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + ethanol (64-17-5) → 2-ethoxy-2-phenylethyl bromide (6589-30-6)

Guidance literature:

With N,N'-dibromo-N,N'-(1,2-ethanediyl)bis(p-toluenesulfonamide); ammonium acetate; at 20 ℃; for 0.05h;

DOI:10.5012/bkcs.2013.34.2.500

Reference yield: 8.8%

ethanol (64-17-5) → 2-ethoxy-2-phenylethyl bromide (6589-30-6) + ethyl 3-ethoxy-3-phenylpropionate (6414-71-7) + ethyl 2-bromo-3-phenyl-propionate (1884-29-3) + (1,2-dibromoethyl)benzene (102921-26-6,93-52-7)

Guidance literature:

With bromine;

DOI:10.1016/S0040-4039(00)92190-7

Reference yield:

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + ethanol (64-17-5) → 2-ethoxy-2-phenylethyl bromide (6589-30-6) + 1-ethoxy-1-phenylethane (3299-05-6)

Guidance literature:

With ammonium bromide; at 30 - 35 ℃; Product distribution; electrooxidation;

DOI:10.1007/BF00961113

upstream raw materials:

Bromoacetaldehyde diethyl acetal

styrene

ethanol

Downstream raw materials:

1-(2-ethoxy-2-phenyl-ethyl)-piperidine

E-1-methyl-4-styryl-benzene

4-methylstilbene

(1-ethoxyvinyl)benzene