(1-ethoxyethenyl)benzene

Base Information

• Chemical Name: (1-ethoxyethenyl)benzene
• CAS No.: 6230-62-2
• Molecular Formula: C10H12O
• Molecular Weight: 148.205

Synonyms:Benzene,(1-ethoxyethenyl);1-ethoxyethenylbenzene;acetophenone ethyl enol ether;1-Ethoxy-1-phenyl-ethen;1-ethoxy-1-phenylethene;Ethyl 1-phenylvinyl ether;

Chemical Property of (1-ethoxyethenyl)benzene

Chemical Property:

• Vapor Pressure: 0.232mmHg at 25°C
• Boiling Point: 214°Cat760mmHg
• Flash Point: 67.9°C
• PSA: 9.23000
• Density: 0.937g/cm³
• LogP: 2.69380

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (1-ethoxyethenyl)benzene

There total 43 articles about (1-ethoxyethenyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

iodobenzene (591-50-4) + trimethyl(1-ethoxylvinyl)tin (112713-84-5) → (1-ethoxyvinyl)benzene (6230-62-2)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; at 95 ℃; for 96h;

DOI:10.1021/jo00297a029

Reference yield: 91.0%

1-Bromoethenyl ethyl ether (100704-20-9) + phenylmagnesium bromide → (1-ethoxyvinyl)benzene (6230-62-2)

Guidance literature:

bis(triphenylphosphine)nickel(II) chloride; In diethyl ether; at 20 ℃; for 1.5h;

Reference yield: 87.0%

dichloromethane (75-09-2) + benzoic acid ethyl ester (93-89-0,99341-95-4) → (1-ethoxyvinyl)benzene (6230-62-2)

Guidance literature:

With titanium tetrachloride; magnesium; In tetrahydrofuran; at 25 ℃; for 1h;

DOI:10.1021/ol047887e

upstream raw materials:

pyridine

1,1,-diethoxy-1-phenylethane

acetyl chloride

2-ethoxy-2-phenylethyl bromide

Downstream raw materials:

1,1-Diphenylethylene

biphenyl

bis(2-oxo-2-phenyl-ethyl)mercury

1-ethoxy-1-phenylethane

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