Methyl 5-formyl-2-methylbenzoate

Base Information

• Chemical Name: Methyl 5-formyl-2-methylbenzoate
• CAS No.: 675148-96-6
• Molecular Formula: C10H10O3
• Molecular Weight: 178.188
• Hs Code.: 2918300090
• Mol file: 675148-96-6.mol

Synonyms:6-Methylisophthalaldehydsaeuremethylester;5-Formyl-2-methyl-benzoic acid methyl ester;Methyl 5-formyl-2-methylbenzoate;3-methoxycarbonyl-4-methyl-benzaldehyde;

Chemical Property of Methyl 5-formyl-2-methylbenzoate

Chemical Property:

• PSA: 43.37000
• LogP: 1.59410
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

98% ^*data from raw suppliers

Methyl5-formyl-2-methylbenzoate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methyl 5-formyl-2-methylbenzoate

There total 12 articles about Methyl 5-formyl-2-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

methanol (67-56-1) + 5-formyl-2-methylbenzoic acid (105650-34-8) → methyl 5-formyl-2-methylbenzoate (675148-96-6)

Guidance literature:

methanol; 5-formyl-2-methylbenzoic acid; With sulfuric acid; at 100 ℃; for 2h; Sealed tube;

With hydrogenchloride; In water; acetone; for 1h;

Reference yield: 76.8%

methyl 5-(hydroxymethyl )-2-methylbenzoate (72985-24-1) → methyl 5-formyl-2-methylbenzoate (675148-96-6)

Guidance literature:

With Dess-Martin periodane; In dichloromethane; at 0 - 20 ℃; for 1.16667h;

Reference yield: 70.0%

2,4-hexadienal (80466-34-8,4488-48-6) + propynoic acid methyl ester (922-67-8) → methyl 5-formyl-2-methylbenzoate (675148-96-6)

Guidance literature:

With acetic acid; dimethyl amine; In ethanol; water; at 80 ℃; for 12h;

DOI:10.1039/c8cc03514h

upstream raw materials:

methanol

carbon monoxide

3-iodo-4-methylbenzaldehyde

5-bromo-2-methylbenzoic acid

Downstream raw materials:

methyl 2-methyl-5-vinylbenzoate

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