2-Ethoxy-1,3,5-trimethoxybenzene

Base Information

• Chemical Name: 2-Ethoxy-1,3,5-trimethoxybenzene
• CAS No.: 69832-53-7
• Molecular Formula: C₁₁H₁₆O₄
• Molecular Weight: 212.246
• DSSTox Substance ID: DTXSID80500331
• Wikidata: Q82351838

Synonyms:2-Ethoxy-1,3,5-trimethoxybenzene;69832-53-7;SCHEMBL23458033;DTXSID80500331

Chemical Property of 2-Ethoxy-1,3,5-trimethoxybenzene

Chemical Property:

• XLogP3: 2.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 5
• Exact Mass: 212.10485899
• Heavy Atom Count: 15
• Complexity: 160

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCOC1=C(C=C(C=C1OC)OC)OC

Technology Process of 2-Ethoxy-1,3,5-trimethoxybenzene

There total 3 articles about 2-Ethoxy-1,3,5-trimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,2,3,5-tetramethoxybenzene (5333-45-9) + propionyl chloride (79-03-8) → 2-Ethoxy-1,3,5-trimethoxybenzol (69832-53-7) + 2-hydroxy-3,4,6-trimethoxypropiophenone (51379-76-1) + 1-(2,3,4,6-tetramethoxyphenyl)propan-1-one (89880-48-8)

Guidance literature:

With aluminium trichloride; In diethyl ether; at 22 ℃; for 2h;

Reference yield:

1,2,3,5-tetramethoxybenzene (5333-45-9) + acetyl chloride (75-36-5) → 1-(2-hydroxy-3,4,6-trimethoxyphenyl)ethanone (7507-98-4) + 1-(2,3,4,6-tetramethoxyphenyl)ethanone (7508-05-6) + 2-Ethoxy-1,3,5-trimethoxybenzol (69832-53-7) + 3-ethoxy-2-hydroxy-4,6-dimethoxyacetophenone (89880-47-7)

Guidance literature:

With aluminium trichloride; In diethyl ether; at 22 ℃; for 2h;

Reference yield:

diethyl sulfate (64-67-5) + 2,4,6-trimethoxyphenol (20491-92-3) → 2-Ethoxy-1,3,5-trimethoxybenzol (69832-53-7)

Guidance literature:

With sodium hydroxide;

DOI:10.1021/jo01327a066

upstream raw materials:

1,2,3,5-tetramethoxybenzene

propionyl chloride

acetyl chloride

diethyl sulfate

Downstream raw materials:

3-Ethoxy-2,4,6-trimethoxybenzaldehyd

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