Bis(trimethylsilyl) phenylboronate

Base Information

Chemical Name:Bis(trimethylsilyl) phenylboronate
CAS No.:7560-51-2
Molecular Formula:C₁₂H₂₃BO₂Si₂
Molecular Weight:266.295
Hs Code.:
DSSTox Substance ID:DTXSID60497351
Wikidata:Q82346803

Synonyms:7560-51-2;Bis(trimethylsilyl) phenylboronate;Boronic acid, phenyl-, bis(trimethylsilyl) ester;trimethyl-[phenyl(trimethylsilyloxy)boranyl]oxysilane;phenylboronic acid bis-tms ester;Bis-trimethylsilyl benzeneboronate;DTXSID60497351;QHKVZAHYVMMIRZ-UHFFFAOYSA-N;Phenylboronic acid, 2TMS derivative

Suppliers and Price of Bis(trimethylsilyl) phenylboronate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of Bis(trimethylsilyl) phenylboronate

Chemical Property:

PSA：18.46000
LogP:3.08480
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:266.1329632
Heavy Atom Count:17
Complexity:214

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:B(C1=CC=CC=C1)(O[Si](C)(C)C)O[Si](C)(C)C

Technology Process of Bis(trimethylsilyl) phenylboronate

There total 2 articles about Bis(trimethylsilyl) phenylboronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1066-40-6
Trimethylsilanol

: 98-80-6
phenylboronic acid

: 7560-51-2
Phenylborsaeure-bis-trimethylsilylester

Guidance literature:: In benzene;

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 98-80-6
phenylboronic acid

: 7560-51-2
Phenylborsaeure-bis-trimethylsilylester

Guidance literature:: Multistep reaction; (i) nBuLi, hexane, PE, (ii) /BRN= 1209232/;

Reference yield: 34.0%

: 7560-51-2
Phenylborsaeure-bis-trimethylsilylester

: 156-87-6
propan-1-ol-3-amine

: 149693-99-2
2-(trimethylsiloxy)-2-phenyl-1,2,3-oxazaborinane

Guidance literature:: In dichloromethane; dropwise addn. of soln. of amine to a soln. of the B-compd. at room temp., stirring for 0.5 h; removal of solvent under vac., recrystn. from CH2Cl2/heptane, elem. anal.;
DOI:10.1016/S0277-5387(00)81537-5