N,N-bis(difluoromethyl)-1,1,1-trifluoromethanamine

Base Information

• Chemical Name: N,N-bis(difluoromethyl)-1,1,1-trifluoromethanamine
• CAS No.: 73551-02-7
• Molecular Formula: C₃H₂F₇N
• Molecular Weight: 185.044
• Mol file: 73551-02-7.mol

Synonyms:

Chemical Property of N,N-bis(difluoromethyl)-1,1,1-trifluoromethanamine

Chemical Property:

• Vapor Pressure: 687mmHg at 25°C
• Boiling Point: 27.7°Cat760mmHg
• Flash Point: °C
• Density: 1.489g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N,N-bis(difluoromethyl)-1,1,1-trifluoromethanamine

There total 4 articles about N,N-bis(difluoromethyl)-1,1,1-trifluoromethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trimethylamine (75-50-3) → perfluorotrimethylamine (432-03-1) + Heptafluorotrimethylamine (73551-02-7) + 1,1-Difluor-N,N-bis(trifluormethyl)methanamin (73563-15-2) + hexafluortrimetylamin

Guidance literature:

With hydrogen fluoride; at -10 ℃; Further byproducts given; electrofluorination;

DOI:10.1016/S0022-1139(00)82579-8

Reference yield:

N,N,N,N,-tetramethylethylenediamine (110-18-9) → perfluorotrimethylamine (432-03-1) + perfluoro(dimethylethylamine) (815-28-1) + Heptafluorotrimethylamine (73551-02-7) + 1,3-bis(trifluoromethyl)-2,2,4,4,5,5-hexafluoro-imidazolidine (74554-48-6)

Guidance literature:

With hydrogen fluoride; at 0 ℃; for 24h; Yield given. Further byproducts given. Yields of byproduct given; current 0.53 A dm^-2; cell voltage 4.7-4.8 V;

DOI:10.1016/s0022-1139(97)00002-x

Reference yield:

trimethylamine (75-50-3) → Heptafluorotrimethylamine (73551-02-7)

Guidance literature:

With cobalt (III) fluoride;

DOI:10.1016/S0040-4020(01)93757-3

upstream raw materials:

trimethylamine

N,N,N,N,-tetramethylethylenediamine

tetramethlyammonium chloride

Refernces

• 1、 Sartori,Velayutham,Ignat'ev,Noel. "Electrochemical fluorination of N,N,N',N'-tetramethylethylenediamine". . p. 1 - 8. Retrieved 2007/10/03.
• 2、 Buerger, H.,Niepel, H.,Pawelke, G.,Frohn, H. J.,Sartori, P.. "HEXA-, HEPTA- UND OCTAFLUORTRIMETHYLAMIN". . p. 231 - 238. Retrieved 2007/10/02.