N-(4-methoxyphenyl)-2-(methylamino)benzamide

Base Information

• Chemical Name: N-(4-methoxyphenyl)-2-(methylamino)benzamide
• CAS No.: 1029-08-9
• Molecular Formula: C15H16 N2 O2
• Molecular Weight: 256.304
• Hs Code.: 2924299090
• DSSTox Substance ID: DTXSID60397504
• Wikidata: Q82198917
• Mol file: 1029-08-9.mol

Synonyms:N-(4-methoxyphenyl)-2-(methylamino)benzamide;1029-08-9;Benzamide,N-(4-methoxyphenyl)-2-(methylamino)-;Oprea1_143884;DTXSID60397504;AKOS008967035;CS-0220571;EN300-06969;Z56945979

Chemical Property of N-(4-methoxyphenyl)-2-(methylamino)benzamide

Chemical Property:

• Vapor Pressure: 2.35E-05mmHg at 25°C
• Boiling Point: 359.6°Cat760mmHg
• Flash Point: 171.3°C
• PSA: 50.36000
• Density: 1.21g/cm³
• LogP: 3.13520
• XLogP3: 3.6
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 4
• Exact Mass: 256.121177757
• Heavy Atom Count: 19
• Complexity: 288

Purity/Quality:

98%,99%, ^*data from raw suppliers

N-(4-METHOXYPHENYL)-2-(METHYLAMINO)BENZAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CNC1=CC=CC=C1C(=O)NC2=CC=C(C=C2)OC

Technology Process of N-(4-methoxyphenyl)-2-(methylamino)benzamide

There total 7 articles about N-(4-methoxyphenyl)-2-(methylamino)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

carbon monoxide (201230-82-2) + 4-methoxy-aniline (104-94-9) + N-methylaniline (100-61-8) → N-(4-methoxyphenyl)-2-(methylamino)benzamide (1029-08-9)

Guidance literature:

With oxygen; copper diacetate; palladium diacetate; acetic acid; potassium iodide; In toluene; acetonitrile; at 70 ℃; for 18h; under 760.051 Torr;

DOI:10.1021/acs.orglett.6b02255

Reference yield: 69.0%

4-methoxy-aniline (104-94-9) + Methyl N-methylanthranilate (85-91-6) → N-(4-methoxyphenyl)-2-(methylamino)benzamide (1029-08-9)

Guidance literature:

4-methoxy-aniline; With trimethylaluminum; In dichloromethane; toluene; at 20 ℃; for 45h;

Methyl N-methylanthranilate; In dichloromethane; toluene; Heating;

DOI:10.1021/jo060070+

Reference yield:

dihydroxy-methyl-borane (13061-96-6) + 2-amino-N-(4-methoxyphenyl)benzamide (20878-54-0) → N-(4-methoxyphenyl)-2-(methylamino)benzamide (1029-08-9)

Guidance literature:

With copper(II) chloride; triethylamine; In methanol; at 20 ℃; for 12h;

DOI:10.1016/j.cclet.2021.09.019

upstream raw materials:

4-methoxy-aniline

Methyl N-methylanthranilate

carbon monoxide

N-methylaniline

Downstream raw materials:

3-(4-methoxyphenyl)-1-methyl-2,3-dihydroquinazolin-4(1H)-one

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