2-Propynoic acid, 3-[2-(trifluoromethyl)phenyl]-, methyl ester

Base Information

Chemical Name:2-Propynoic acid, 3-[2-(trifluoromethyl)phenyl]-, methyl ester
CAS No.:841205-62-7
Molecular Formula:C11H7F3O2
Molecular Weight:228.171
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Propynoic acid, 3-[2-(trifluoromethyl)phenyl]-, methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of 2-Propynoic acid, 3-[2-(trifluoromethyl)phenyl]-, methyl ester

There total 3 articles about 2-Propynoic acid, 3-[2-(trifluoromethyl)phenyl]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 67-56-1
methanol

: 201230-82-2
carbon monoxide

: 704-41-6
1-ethynyl-2-(trifluoromethyl)benzene

: 841205-62-7
methyl 3-(2-(trifluoromethyl)phenyl)propiolate

Guidance literature:: With bis(benzonitrile)palladium(II) chloride; silver trifluoromethanesulfonate; N-{(1E,2E)-2-[(2,6-diisopropylphenyl)imino]acenaphthenylidene}-2,6-diisopropylaniline; p-benzoquinone; In tetrahydrofuran; at 20 ℃; for 42h; under 3000.3 Torr; Autoclave; Schlenk technique; Inert atmosphere;
DOI:10.1002/adsc.201600521

Reference yield: 16.0%

: 444-29-1
2-iodo(trifluoromethyl)benzene

: 922-67-8
propynoic acid methyl ester

: 841205-62-7
methyl 3-(2-(trifluoromethyl)phenyl)propiolate

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; triethylamine; zinc dibromide; In tetrahydrofuran;
DOI:10.1002/ejoc.200400881