1-Ethyl-2,3-dimethylimidazolium chloride

Base Information

• Chemical Name: 1-Ethyl-2,3-dimethylimidazolium chloride
• CAS No.: 92507-97-6
• Molecular Formula: C7H13 N2 . Cl
• Molecular Weight: 160.647
• Hs Code.: 2933290090
• European Community (EC) Number: 627-934-7
• DSSTox Substance ID: DTXSID90370148
• Mol file: 92507-97-6.mol

Synonyms:1-Ethyl-2,3-dimethylimidazolium chloride;92507-97-6;1-Ethyl-2,3-dimethyl-3-imidazolium Chloride;1-Ethyl-2,3-dimethyl-1H-imidazol-3-ium chloride;1-ethyl-2,3-dimethylimidazol-3-ium;chloride;MFCD03093290;1-ethyl-2,3-dimethylimidazol-3-ium chloride;1-ETHYL-2,3-DIMETHYLIMIDAZOLIUMCHLORIDE;SCHEMBL385497;DTXSID90370148;NUJYCYLTUXYHQU-UHFFFAOYSA-M;AC8650;AKOS027320322;1,2-dimethyl-3-ethylimidazolium chloride;BS-18249;SY060847;1-ethyl-2,3-dimethyl-imidazolium chloride;CS-0152006;1-Ethyl-2,3-Dimethylimidazolium Chloride (T);A860062;1-Ethyl-2,3-dimethylimidazolium chloride, >=97.0% (T)

Chemical Property of 1-Ethyl-2,3-dimethylimidazolium chloride

Chemical Property:

• Melting Point: 182-184 °C
• PSA: 8.81000
• LogP: -2.35510
• Storage Temp.: Inert atmosphere,Room Temperature
• Sensitive.: Moisture Sensitive
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 160.0767261
• Heavy Atom Count: 10
• Complexity: 92.9

Purity/Quality:

97% ^*data from raw suppliers

1-Ethyl-2,3-dimethyl-1H-imidazol-3-iumchloride 95+% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: CCN1C=C[N+](=C1C)C.[Cl-]
• Uses: It is used reaction media for chemical processes.

Technology Process of 1-Ethyl-2,3-dimethylimidazolium chloride

There total 2 articles about 1-Ethyl-2,3-dimethylimidazolium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

1-Ethyl-2-methyl-3-methylimidazolium bromide (98892-76-3) → 1-ethyl-2,3-dimethyl-3H-imidazole-1-ium chloride (92507-97-6)

Guidance literature:

With anion exchange resin (Ambersep 900-Cl); In water;

Reference yield:

1,2-dimethyl-1H-imidazole (1739-84-0) + chloroethane (75-00-3) → 1-ethyl-2,3-dimethyl-3H-imidazole-1-ium chloride (92507-97-6)

Guidance literature:

In acetonitrile; for 48h; Reflux;

DOI:10.1134/S0036024418120245

Reference yield: 71.0%

1-ethyl-2,3-dimethyl-3H-imidazole-1-ium chloride (92507-97-6) + N-(4-methoxybenzylidene)-p-toluenesulfonamide (14674-38-5) → (2-(3-ethyl-1-methyl-1H-imidazol-3-ium-2-yl)-1-(4-methoxyphenyl)ethyl)(tosyl)amide

Guidance literature:

1-ethyl-2,3-dimethyl-3H-imidazole-1-ium chloride; With caesium carbonate; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;

N-(4-methoxybenzylidene)-p-toluenesulfonamide; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

DOI:10.1021/acs.joc.7b00807

upstream raw materials:

1-Ethyl-2-methyl-3-methylimidazolium bromide

1,2-dimethyl-1H-imidazole

chloroethane

Downstream raw materials:

1-ethyl-2,3-dimethylimidazolium bis(trifluoromethylsulfonyl)imide

1-ethyl-2,3-dimethylimidazolium iodide