S,S-Dipropyl-N-(p-tolylsulfonyl)sulfimine

Base Information

• Chemical Name: S,S-Dipropyl-N-(p-tolylsulfonyl)sulfimine
• CAS No.: 17626-99-2
• Molecular Formula: C13H21NO2S2
• Molecular Weight: 287.447
• NSC Number: 118139
• DSSTox Substance ID: DTXSID00938778
• Nikkaji Number: J1.264.403E
• Wikidata: Q82915186
• Mol file: 17626-99-2.mol

Synonyms:17626-99-2;NSC118139;DTXSID00938778;NSC-118139;N-(Dipropyl-lambda~4~-sulfanylidene)-4-methylbenzene-1-sulfonamide

Chemical Property of S,S-Dipropyl-N-(p-tolylsulfonyl)sulfimine

Chemical Property:

• Vapor Pressure: 2.42E-07mmHg at 25°C
• Boiling Point: 434.4°Cat760mmHg
• Flash Point: 216.5°C
• Density: 1.16g/cm³
• XLogP3: 4.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 6
• Exact Mass: 287.10137126
• Heavy Atom Count: 18
• Complexity: 355

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCS(=NS(=O)(=O)C1=CC=C(C=C1)C)CCC

Technology Process of S,S-Dipropyl-N-(p-tolylsulfonyl)sulfimine

There total 4 articles about S,S-Dipropyl-N-(p-tolylsulfonyl)sulfimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

propyl sulfide (111-47-7) + toluene-4-sulfonamide (70-55-3) → S,S-dipropyl-N-(toluene-4-sulfonyl)-sulfimide (17626-99-2)

Guidance literature:

propyl sulfide; toluene-4-sulfonamide; With [bis(acetoxy)iodo]benzene; In dichloromethane; for 0.5h;

With triethylamine; for 1h;

DOI:10.1080/00397919908086608

Reference yield:

propyl sulfide (111-47-7) + N-bromo-N-potassio-p-toluenesulfonamide (70284-20-7) → dipropyl sulfoxide (4253-91-2) + S,S-dipropyl-N-(toluene-4-sulfonyl)-sulfimide (17626-99-2) + toluene-4-sulfonamide (70-55-3)

Guidance literature:

With Britton-Robinson buffer; In methanol; water; at 20 ℃; Rate constant; Mechanism; Product distribution; NaOH, other pH values; also in unbuffered solution;

Reference yield:

propyl sulfide (111-47-7) + chloroamine-T (127-65-1) → S,S-dipropyl-N-(toluene-4-sulfonyl)-sulfimide (17626-99-2)

Guidance literature:

With ethanol;

DOI:10.1021/ja01243a015

upstream raw materials:

propyl sulfide

chloroamine-T

N-bromo-N-potassio-p-toluenesulfonamide

toluene-4-sulfonamide

Downstream raw materials:

propyl sulfide