1,3-Bis(2-bromoethoxy)-5-iodobenzene

Base Information

Chemical Name:1,3-Bis(2-bromoethoxy)-5-iodobenzene
CAS No.:916905-33-4
Molecular Formula:C10H11Br2IO2
Molecular Weight:449.909
Hs Code.:
DSSTox Substance ID:DTXSID10581294
Nikkaji Number:J2.393.022F
Wikidata:Q82472370

Synonyms:1,3-Bis(2-bromoethoxy)-5-iodobenzene;916905-33-4;DTXSID10581294

Suppliers and Price of 1,3-Bis(2-bromoethoxy)-5-iodobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 1,3-Bis(2-bromoethoxy)-5-iodobenzene

Chemical Property:

XLogP3:4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:6
Exact Mass:449.81500
Heavy Atom Count:15
Complexity:156

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=C(C=C(C=C1OCCBr)I)OCCBr

Technology Process of 1,3-Bis(2-bromoethoxy)-5-iodobenzene

There total 4 articles about 1,3-Bis(2-bromoethoxy)-5-iodobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 64339-43-1
5-iodoresorcinol

: 106-93-4
ethylene dibromide

: 916905-33-4
1,3-bis(2-bromoethoxy)-5-iodobenzene

Guidance literature:: With potassium carbonate; In acetone; for 36h; Heating;
DOI:10.1021/jo0617868 DOI:10.1021/ja064742p

Reference yield:

: 25245-27-6
1-iodo-3,5-dimethoxybenzene

: 916905-33-4
1,3-bis(2-bromoethoxy)-5-iodobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / aq. HI / 24 h / Heating

2: 62 percent / K₂CO₃ / acetone / 36 h / Heating

With hydrogen iodide; potassium carbonate; In acetone;
DOI:10.1021/ja064742p

Reference yield:

: 89981-17-9
3,5-dimethoxy-1-phenylmagnesium chloride

: 916905-33-4
1,3-bis(2-bromoethoxy)-5-iodobenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / iodine / tetrahydrofuran / 2 h / 0 °C

2: 97 percent / aq. HI / 24 h / Heating

3: 62 percent / K₂CO₃ / acetone / 36 h / Heating

With hydrogen iodide; iodine; potassium carbonate; In tetrahydrofuran; acetone;
DOI:10.1021/ja064742p