Benzenecarbothioic acid, 4-methoxy-, S-(4-methoxyphenyl) ester

Base Information

Chemical Name:Benzenecarbothioic acid, 4-methoxy-, S-(4-methoxyphenyl) ester
CAS No.:98098-60-3
Molecular Formula:C15H14O3S
Molecular Weight:274.34
Hs Code.:

Synonyms:Benzenecarbothioic acid,4-methoxy-,S-(4-methoxyphenyl) ester;4-methoxy-thiobenzoic acid S-(4-methoxy-phenyl ester);S-(4-methoxyphenyl) 4-methoxybenzothioate;4-Methoxy-thiobenzoesaeure-S-(4-methoxy-phenylester);

Suppliers and Price of Benzenecarbothioic acid, 4-methoxy-, S-(4-methoxyphenyl) ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenecarbothioic acid, 4-methoxy-, S-(4-methoxyphenyl) ester

Chemical Property:

PSA：60.83000
LogP:3.63630

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzenecarbothioic acid, 4-methoxy-, S-(4-methoxyphenyl) ester

There total 7 articles about Benzenecarbothioic acid, 4-methoxy-, S-(4-methoxyphenyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 696-63-9
4-Methoxybenzenethiol

: 696-62-8
para-iodoanisole

: 82102-37-2
9-methyl-9H-fluorene-9-carbonyl chloride

: 98098-60-3
S-(4-methoxyphenyl) 4-methoxybenzothioate

Guidance literature:: With N-Methyldicyclohexylamine; sodium acetate; palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether; bis(dibenzylideneacetone)-palladium⁽⁰⁾; tri tert-butylphosphoniumtetrafluoroborate; In 1,2-dimethoxyethane; at 85 ℃; for 18h; chemoselective reaction;
DOI:10.1021/ol400138m

Reference yield: 83.0%

: 696-63-9
4-Methoxybenzenethiol

: 100-07-2
4-methoxy-benzoyl chloride

: 98098-60-3
S-(4-methoxyphenyl) 4-methoxybenzothioate

Guidance literature:: With pyridine; In acetonitrile; at 0 - 25 ℃; for 2h;
DOI:10.1002/chem.201705576

Reference yield: 80.0%

: 104-92-7
1-bromo-4-methoxy-benzene

: 696-63-9
4-Methoxybenzenethiol

: 82102-37-2
9-methyl-9H-fluorene-9-carbonyl chloride

: 98098-60-3
S-(4-methoxyphenyl) 4-methoxybenzothioate

Guidance literature:: 1-bromo-4-methoxy-benzene; 4-Methoxybenzenethiol; With bis(benzonitrile)palladium(II) dichloride; sodium acetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; Inert atmosphere; Glovebox;

9-methyl-9H-fluorene-9-carbonyl chloride; With N-Methyldicyclohexylamine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; tri tert-butylphosphoniumtetrafluoroborate; at 120 ℃; for 24h; Inert atmosphere; Glovebox;
DOI:10.1021/jo5009965